CIE iGCSE Co-Ordinated Science C12.4 Separation and purification Exam Style Questions Paper 2
Question
Which graph shows the temperature change when an impure, solid substance is heated?

▶️ Answer/Explanation
✅ Answer: (A)
Question
A sample of water contains two useful substances, insoluble chalk and a soluble salt.
Which two processes are used to individually separate the insoluble chalk from the soluble salt and from the water?
A. distillation and chromatography
B. distillation and crystallisation
C. filtration and chromatography
D. filtration and crystallisation
▶️ Answer/Explanation
Crystallisation is then used to separate the dissolved soluble salt from the water by evaporating the solvent.
✅ Answer: (D)
Question
An aqueous salt solution contains an insoluble impurity.
Which processes are used to obtain pure salt crystals?
A. distillation then crystallisation
B. distillation then chromatography
C. filtration then crystallisation
D. filtration then chromatography
▶️ Answer/Explanation
The filtrate is then evaporated/cooled through crystallisation to grow pure salt crystals from solution.
✅ Answer: (C)
Question
Hexane and octane are liquid hydrocarbons that mix together.
Which apparatus is used to separate a mixture of these two liquids?

▶️ Answer/Explanation
This requires a fractionating column fitted above the flask, allowing vapours to separate as they condense at different heights — shown in apparatus D.
✅ Answer: (D)
Question
A mixture of solid sulfur and solid sodium chloride is added to water and stirred.
Sulfur is insoluble in water. Sodium chloride is soluble in water.
Which processes are used to obtain pure sodium chloride from the mixture?
A. distillation then chromatography
B. distillation then crystallisation
C. filtration then chromatography
D. filtration then crystallisation
▶️ Answer/Explanation
The filtrate, a sodium chloride solution, is then heated to evaporate water until saturated, and cooled to allow crystals of sodium chloride to form — this is crystallisation.
Distillation and chromatography are not needed here, since the goal is to recover a dissolved solid, not to separate a liquid mixture or coloured substances.
✅ Answer: (D)
